Front contact photo-electrochemical H-Cell setup (redox.me)

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  Activation furnance for electrochemical sensors

  The activation furnance is a device used for curing individual sensors of the AC1 type. At a defined temperature (up to 1000 °C) depending on the electrode and sensor materials. When the sensor is cured, the surface of the electrodes is cleaned from surface oxides and organic impurities, which results in regeneration of the sensor or its activation. In this way, for example, old sensors with immobilized enzyme layers can be cured for reuse – see example at the end ot the document.

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  ZIVE SP1 – potentiostat/galvanostat/ZRA

  • Potentiostat/galvanostat/ZRA at affordable price
  • Control voltage range: ±10V
  • Control current range:9 ranges, 10nA~1A (10nA with gain)

   

  Application Battery Super capacitor Fuel cell Corrosion Sensor Solar cell Other Echem experiments Features economical high quality potentiostat/galvanostat/impedance analyzer compact size with full functions ±10V@1Amp control range wide current ranges(1A to 10nA) for various applications built-in FRA : enables EIS tests by using software 14 EIS techniques capability including multisine capable of multitude of applications – corrosion, general electrochemistry, sensor, battery, fuel cell, supercapacitor, solar cell, etc. bipolar pulse capability voltage pulse or current pulse charge/discharge test(GSM,CDMA etc.), sine wave function for ripple simulation withenergysoftwarepackage & pulse plating available high speed data sampling time – 2usec or 3usec depending on data point number iR compensation and measurement 3 measurement/control voltage ranges & 9 measurement/control current ranges internal 542,000 data point storage & continuing experiment regardless of PC failure. multichannel configuration available free software upgrade Experimental Techniques Basic techniques Potentiostatic Galvanostatic Double step potentiostatic Double step galvanostatic OCP measurement Potential sweep Current sweep Cyclic voltammetry Fast potential sweep Potentiostatic Ru measurement Galvanostatic Ru measurement Advanced Software Package(Included) EIS software package(EISe) – Potentiostat EIS – Galvanostatic EIS – Pseudo galvanostatic EIS – OCP* EIS – Potentiodynamic PEIS – Galvanodynamic GEIS – Poteniodynamic HFR – Galvanodynamic HFR – Potentiostatic HFR monitor – Galvanostatic HFR monitor – Multisine potentiostatic EIS – Multisine galvanostatic EIS – Intermittent potentiostatic EIS – Intermittent galvanostatic EIS (*) The system measures open circuit potential before each frequency change and applies AC sine wave on this potential. Corrosion software package(CORe) – Tafel(Tafel experiment) – Rp(Polarization resistance) – RpEc trend – PDYN(Potentiodynamic) – CYPOL(Cyclic polarization resistance) – GDYN(GalvanoDynamic) – Reactivation – Galvanic corrosion – Potentiostatic ECN – Galvanostatic ECN – ZRA mode ECN Energy software package(BATe) a) Battery test technique – CC/CV testforcycle life test of lithium battery – CC/CC tet forcyclelifetestofNiCd or NiMH battery – Discharging test – EVS(electrochemical voltage spectroscopy) – Variable scan rate CV – Potentiostatic IV curve – Galvanostatic IV curve – Steady state CV – PITT(Potentiostatic intermittent titration technique) test – GITT(Galvanostatic intermittent titration technique) test – Pulse mode is available for GSM & CDMA profile. Pulse shape profile can be measured by user’s demand. b) Control mode – Charge : CC, CC-CV, pulse, sine wave – Discharge : CC, CP, CR, pulse, sine wave c) Cut-off condition – Time, voltage, current, power, auxV etc. – Various battery charge/discharge test is available including pulse discharge for GSM, CDMA application Electrochemical analysis software package(EASe) a) Step techniques – CA(Chronoamperometry) – CC(Chronocoulometry) – CP(Chronopotentiometry) b) Sweep techniques – LSV(Linear sweep voltammetry) – SDV(Sampled DC voltammetry) – Fast CV – Fast LSV c) Pulsed techniques – DPV(Differential pulse voltammetry) – SWV(Square wave voltammetry) – DPA(Diff.pulse amperometry) – NPV(Normal pulse voltammetry) – RNPV(Reverse normal pulse voltammetry) – DNPV(Differential normal pulse voltammetry)

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• 

  Membrane Capacitive Deionization configurable cell (redox.me)

  Membrane Capacitive Deionization (MCDI) configurable cell has been designed to conduct research on removal of charged ionic species from aqueous or organic solutions (i.e., Desalination/Demineralization) via electrostatic (i.e., non-Faradaic) or electrochemical (redox) interactions. The MCDI cell contains two graphite current collectors that can serve as polarization electrodes. However, if the electrode material is the subject of research, it should be applied to an additional current collector, such as graphite paper or metal felt (not included in the product). Different electrode materials can be installed on both sides of the cell. If the thickness of these electrodes exceeds 250 micrometers, different gaskets are required. In such a case, please contact us for a solution.

  The cell is designed in such a way that replacing the electrodes does not require removing the membranes or flow fields. It is enough to unscrew the plungers on both sides and replace the electrodes. In the standard configuration, the liquid in the main channel and side channels flows through the flow field cut from PEEK. However, these can be replaced with a porous material such as felt or a battery spacer, which will allow fluid flow. If work with materials of dimensions different from those listed in the specification is required, we can supply seals of different thicknesses or customize the cell. The cell allows for the installation of one or two ion-exchange membranes (not included in the setup). Their thickness is not critical, and it is not necessary to adjust the thickness of the membrane gaskets pressing them. The cell elements are constructed with inert materials to the sample (PEEK). It well fits aqueous (FKM gaskets and O-rings) and organic solvent (FFKM gaskets and O-rings) electrolyte requirements. The construction of the cell is gas-tight.

   

  Application note:
  MCDI cell can be configured to allow the following cell architectures:

  1. Flow-by CDI consisting of: (i) two porous carbon or metal based current collectors coated with capacitive (e. non-Faradaic) material, and (ii) a main flow field enabling the feed water to be transported between electrodes. In this configuration, side flow fields and membranes are not installed.  
  2. Membrane CDI consisting of: (i) two porous carbon or metal based current collectors coated with capacitive (e. non-Faradaic) material, (ii) two ion-exchange membranes (cation exchange membrane and anion exchange membrane) separating electrodes from the main flow field, and (iii) a main flow field enabling the feed water to be transported between electrodes. In this configuration, side flow fields are typically not installed. However, there are cases where installing both side flow fields is justified. All the graphics included in the product page refer to that configuration.
  3. Inverted CDI consisting of: (i) two porous carbon or metal based current collectors coated with capacitive (e. non-Faradaic) material where anode is treated for net negative surface charge and a cathode is treated for net positive surface charge, and (ii) a main flow field enabling the feed water to be transported between electrodes. In this configuration, side flow fields and membranes are not installed.  
  4. Flow-electrode CDI consisting of: (i) two porous carbon or metal based current collectors with flowing electrodes made of capacitive (e. non-Faradaic) carbon suspension, (ii) two ion-exchange membranes (cation exchange membrane and anion exchange membrane) separating electrodes from the flow chamber, (iii) a main flow field enabling the feed water to be transported between electrodes, and (iv) two side flow fields for liquid electrodes. All the graphics included in the product page refer to that configuration.
  5. Hybrid CDI consisting of: (i) a Faradaic (e. battery) electrode for cation adsorption/desorption, (ii) a capacitive (i.e. non-Faradaic) electrode for anion adsorption/desorption, (iii) an anion exchange membrane placed adjacent to the capacitive electrode, and (iv) a main flow field enabling the feed water to be transported between electrodes. In this configuration, side flow fields and a cation-exchange membrane are not installed.  
  6. Cation intercalation desalination consisting of: (i) two porous carbon or metal based current collectors coated with Faradaic cation intercalation materials, (ii) an anion exchange membrane separating electrodes, and (iii) a main flow field enabling the feed water to be transported between electrodes. In this configuration, one side flow field and cation-exchange membrane are not installed.  
  7. Desalination battery consisting of: (i) two porous carbon or metal based current collectors coated with redox (e. Faradaic) material (one for cation adsorption/desorption and the other for anion adsorption/desorption), and (ii) a main flow field enabling the feed water to be transported between electrodes. In this configuration, side flow fields and membranes are not installed.  

   

  Specification:
  tubing size: 4 mm OD
  fitting type: push-in, M5 male
  electrode size: 60 mm x 60 mm (36 cm²)
  recommended total electrode thickness: 200-250 µm
  membrane size: 70 mm x 85 mm
  maximum operating pressure: 20 bar
  maximum operating temperature 150 ºC

  Intrastat data:
  HS Code: 90278080
  Country of Origin: Sweden
  NET weight: 1300 g

   

  Product includes:
  2 x stand, anodized aluminum
  2 x plunger holder, SS 316L
  2 x PEEK plunger
  2 x tantalum current collector
  2 x graphite current collector
  1 x threaded end plate, SS 316L
  1 x unthreaded end plate, SS 316L
  1 x PEEK outer cell body
  1 x PEEK inner cell body
  1 x set of fittings
  2 x female banana connectors, 4 mm dia.
  1 x PEEK main flow field, 0.5 mm thick
  2 x PEEK side flow field, 0.5 mm thick
  1 x set of gaskets (FKM or FFKM) including:

  1 x main flow gasket, 0.5 mm thick
  2 x membrane gasket, 0.25 mm thick
  2 x side flow gasket, 0.5 mm thick
  2 x electrode gasket, 0.25 mm thick

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• 

  Basic electrochemical cell setup (redox.me)

  This is a stationary solution basic electrochemical cell for measurements of electrodes in a form of:

  a) rod/disc (6 mm dia.),

  b) thin film deposited on a flat substrate (using a wire clip) and

  c) membrane (using a wire clip).

   

  The working, counter, and reference electrodes are mounted in a top casing either in 2-, or 3-electrode setup. The cell elements are constructed with materials that are inert to the sample (glass and PEEK). It well fits aqueous (FKM/EPDM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. The construction is gas-tight and can be used when the removal and exclusion of contaminants such as oxygen and water is required by bubbling of an inert gas through the electrolyte. The cell chamber is available in several material variants here (glass, PTFE, PEEK)

   

  Application note:
  The reference electrode tip should be placed at the level of working electrode center. This will ensure a low potential drop throughout the electrolyte solution for low-current experiment. Various auxiliary electrodes are suitable for this cell including metal wire and metal foil electrodes as well as graphite rod. The bubbling of gas through the solution must be stopped prior to experiment.

   

  Specification:
  maximum electrolyte volume: 50 mL
  electrode plug diameter: 6 mm
  number of electrode slots: 3

   

  Intrastat data:
  HS Code: 90309000
  Country of Origin: Sweden
  NET weight: 200 g

   

  Setup includes:

  Item	Qty	B-A-BEC-50	B-O-BEC-50
  BEC 50 mL – Basic Electrochemical Cell	1	C-A-BEC-50	C-O-BEC-50
  Metal wire auxiliary electrode – 50HX15 0.6/250 mm, platinum (99,9%), 1 mm dia. gold plated pin	1	E-A-50HX15_Pt-1mm	E-O-50HX15_Pt-1mm
  Silver / Silver Chloride Reference Electrode – Ag/AgCl 70 mm	1	E-Ag/AgCl_70
  Non-aqueous Silver / Silver Ion Reference Electrode – Ag/Ag+ 70 mm	1		E-Ag/Ag+_70
  Working disk electrode – 2 mm dia., PEEK BODY 6 mm dia. – 70 mm, glassy carbon	1	E-A-DISK_GC-70	E-O-DISK_GC-70
  10 pcs of Tantalum wire clip with septum plug 0.6 mm dia., 60 mm long	1	E-A-Ta_CLIP-0.6/60-10p	E-O-Ta_CLIP-0.6/60-10p

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