Hanging Platinum Drop Electrode

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  Basic Sample Holder – metal contact, 4 mm max. thickness (redox.me)

  Basic Sample Holder with a metal contact works as an electrical conductor between an electrode material (free-standing or deposited on a substrate) and an external circuit. This holder consists of PEEK body, pure Tantalum, Stainless Steel 316L, Titanium, Copper or Nickel metal electrical contact, and PEEK screw to fix the electrode. It is compatible with most of inorganic and organic based plates, free-standing membranes or thin films deposited on flexible and rigid substrates. A maximum thickness of the sample is 4 mm. Tantalum is known to be inert to practically all organic and inorganic compounds. Tantalum’s corrosion resistance is very similar to that of glass, as both are unsuitable for use in hydrofluoric acid and strong hot alkali applications. Therefore, in those cases, we recommend the other wire contact variant.  The metal contact can be fully immersed in the electrolyte. 

   

  Application note
  Generally, the electrode is fabricated by fixing the electrochemical active sample into the holder using a screw. Such electrode is immersed in the ion-conducting solution as a working electrode or counter electrode. An electric current is passed between the working electrode and the counter electrode for a certain amount of time. Metal wire contact is permanently installed in the PEEK body. The holder is designed to be used multiple times. The holder should be cleaned prior to the installation of electrode material.

   

  Specification
  holder body material: PEEK
  rod diameter: 6 mm
  contact material: Ta, SS 316L, Ti, Cu or Ni
  contact wire diameter: 0.6 mm
  contact wire total length: 110 mm
  holder length: 70 mm
  maximum sample thickness: 4 mm

   

  Intrastat data
  HS Code: 90309000
  Country of Origin: Sweden
  NET weight: 100 g

   

  Product includes
  1 x Basic Sample Holder
  1 x PEEK M3 screw
  1 O-Ring (FKM for aqueous or FFKM for organic electrolytes)

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  ZIVE SP1 – potentiostat/galvanostat/ZRA

  • Potentiostat/galvanostat/ZRA at affordable price
  • Control voltage range: ±10V
  • Control current range:9 ranges, 10nA~1A (10nA with gain)

   

  Application Battery Super capacitor Fuel cell Corrosion Sensor Solar cell Other Echem experiments Features economical high quality potentiostat/galvanostat/impedance analyzer compact size with full functions ±10V@1Amp control range wide current ranges(1A to 10nA) for various applications built-in FRA : enables EIS tests by using software 14 EIS techniques capability including multisine capable of multitude of applications – corrosion, general electrochemistry, sensor, battery, fuel cell, supercapacitor, solar cell, etc. bipolar pulse capability voltage pulse or current pulse charge/discharge test(GSM,CDMA etc.), sine wave function for ripple simulation withenergysoftwarepackage & pulse plating available high speed data sampling time – 2usec or 3usec depending on data point number iR compensation and measurement 3 measurement/control voltage ranges & 9 measurement/control current ranges internal 542,000 data point storage & continuing experiment regardless of PC failure. multichannel configuration available free software upgrade Experimental Techniques Basic techniques Potentiostatic Galvanostatic Double step potentiostatic Double step galvanostatic OCP measurement Potential sweep Current sweep Cyclic voltammetry Fast potential sweep Potentiostatic Ru measurement Galvanostatic Ru measurement Advanced Software Package(Included) EIS software package(EISe) – Potentiostat EIS – Galvanostatic EIS – Pseudo galvanostatic EIS – OCP* EIS – Potentiodynamic PEIS – Galvanodynamic GEIS – Poteniodynamic HFR – Galvanodynamic HFR – Potentiostatic HFR monitor – Galvanostatic HFR monitor – Multisine potentiostatic EIS – Multisine galvanostatic EIS – Intermittent potentiostatic EIS – Intermittent galvanostatic EIS (*) The system measures open circuit potential before each frequency change and applies AC sine wave on this potential. Corrosion software package(CORe) – Tafel(Tafel experiment) – Rp(Polarization resistance) – RpEc trend – PDYN(Potentiodynamic) – CYPOL(Cyclic polarization resistance) – GDYN(GalvanoDynamic) – Reactivation – Galvanic corrosion – Potentiostatic ECN – Galvanostatic ECN – ZRA mode ECN Energy software package(BATe) a) Battery test technique – CC/CV testforcycle life test of lithium battery – CC/CC tet forcyclelifetestofNiCd or NiMH battery – Discharging test – EVS(electrochemical voltage spectroscopy) – Variable scan rate CV – Potentiostatic IV curve – Galvanostatic IV curve – Steady state CV – PITT(Potentiostatic intermittent titration technique) test – GITT(Galvanostatic intermittent titration technique) test – Pulse mode is available for GSM & CDMA profile. Pulse shape profile can be measured by user’s demand. b) Control mode – Charge : CC, CC-CV, pulse, sine wave – Discharge : CC, CP, CR, pulse, sine wave c) Cut-off condition – Time, voltage, current, power, auxV etc. – Various battery charge/discharge test is available including pulse discharge for GSM, CDMA application Electrochemical analysis software package(EASe) a) Step techniques – CA(Chronoamperometry) – CC(Chronocoulometry) – CP(Chronopotentiometry) b) Sweep techniques – LSV(Linear sweep voltammetry) – SDV(Sampled DC voltammetry) – Fast CV – Fast LSV c) Pulsed techniques – DPV(Differential pulse voltammetry) – SWV(Square wave voltammetry) – DPA(Diff.pulse amperometry) – NPV(Normal pulse voltammetry) – RNPV(Reverse normal pulse voltammetry) – DNPV(Differential normal pulse voltammetry)

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  Working Disk Electrode – PEEK body 6 mm dia., 70 mm long (redox.me)

  This is a Standard Working Electrode in which a disk of electrode material (glassy carbon, gold, platinum, silver, boron-doped diamond, palladium, titanium, and copper) is embedded into the PEEK body by a compressed PTFE or PEEK sleeve. It well fits aqueous and organic solvent electrolyte requirements. If you need a different disk material, please contact us.

   

  Application note
  The disk electrode is immersed in the ion-conducting solution as a working electrode. An electric current is passed between the working electrode and the counter electrode for a certain amount of time. After the experiment, the electrode should be washed several times with ethanol or isopropanol. If the disk electrode was used as a current collector with other electrode material, or when there are visible traces of material absorption, it should be polished down to the mirror surface after the experiment is completed. Store the working disk electrode in the glass tube sealed with an O-ring (all included in the package). Instruction on maintenance is provided on the Electrode Polishing Kit product page. 

   

  Specification

  disk diameter: 2, 3, 4 or 5 mm
  disk length: 1.5 mm for BDD, 3 mm for the rest
  body material: PEEK with PTFE or PEEK sleeve
  body diameter: 6 mm
  body length: 70 mm

   

  Intrastat data
  HS Code: 85451900
  Country of Origin: Sweden
  NET weight: 100 g

   

  Product includes
  1x working disk electrode
  1x O-ring
  1x glass tube

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  Activation furnance for electrochemical sensors

  The activation furnance is a device used for curing individual sensors of the AC1 type. At a defined temperature (up to 1000 °C) depending on the electrode and sensor materials. When the sensor is cured, the surface of the electrodes is cleaned from surface oxides and organic impurities, which results in regeneration of the sensor or its activation. In this way, for example, old sensors with immobilized enzyme layers can be cured for reuse – see example at the end ot the document.

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