Category
- NEW PRODUCTS
- CUSTOMER SERVICES
- Custom made glass products
- Custom made and Modified Screen Printed Electrodes
- Sensors and electrodes
- Cables and connectors
- Cell
- Spectro, Photo, Raman – electrochemical cells
- Membrane Capacitive Deionization configurable cell
- NREL High-Pressure Low-Temperature Electrolysis Cell
- High-Pressure (25 bar) Single-Compartment Electrochemical Cell
- Stirrers
- Pumps
- Kits & Sets
- Minithermostat
- Modular PEM Electrolyzer Test Station
- Measurements of battery and supercapacitor materials
- Potentiostats
- Manual Screen Printer
- Accessories
- Discounted SPEs (at a reduced price with visual defects/inconsistancies, but fully functional)
NREL High-Pressure Low-Temperature Electrolysis Cell (redox.me)
Developed by National Renewable Energy Laboratory (NREL) High-Pressure Low-Temperature Electrolysis (LTE) Cell is on open-source cell hardware designed for repeated reassembly. This work was planned and funded by the U.S. Department of Energy’s H2NEW consortium.
Redox.me offers a 25 cm² PEM variant produced based on the technical documentation from NREL, as well as other variants developed by redox.me according to NREL guidelines. In the former, the flow field pattern is directly translated from 25 cm² PEM variant. The dissemination of these products aims to facilitate easy access to this equipment for a wide range of users. However, if you have the capability to produce the 25 cm² PEM variant on your own, we encourage you to use the open-source files. It may turn out that if you have access to your own technical resources, this will be a more cost-effective option. 3D CAD models and 2D technical drawings for variant 25 cm² PEM are available for download.
High pressure LTE operation can reduce operating costs, as it is more efficient to produce electrochemically pressurized hydrogen compared to using downstream mechanical compressors. However, the cell is also compatible with ambient pressure LTE.
The cell can accommodate porous transport layers of varying thicknesses. To achieve this, the number of gaskets on each side of the cell can be increased, providing a larger volume for the porous transport layer.
One benefit of the smaller surface area variants (1 cm² and 4 cm²) is their compatibility for testing with a potentiostat and booster. In these cases, the current levels are typically within the acceptable range for most boosters. However, for larger active surfaces with current densities up to 6 A/cm², a high-power programmable DC power supply may be required.
Application note:
The documents and drawings linked below outline the design of low-temperature electrolysis hardware that is intended to meet leak testing standards as per ASME B31.1. They also provide comprehensive cell assembly instructions and a procedure for performance benchmarking. The responsibility for safe operation at both ambient and elevated pressures lies solely with the end user, and each individual cell should be assessed on a case-by-case basis. The sealing effectiveness may be influenced by factors such as machining quality, components used in cell assembly, operating conditions, and the operational history. Pressure operations should only be conducted on qualified test stands by trained operators.
Specification:
- cell
active area: 25 cm², 4 cm² or 1 cm² (other on request)
maximum verified working pressure: 30 bar
flow field design: triple serpentine (other on request) - temperature sensor
sensor type: Pt100 x2 (100 W at 0 ºC)
construction: Wire-Wound, 10 mm tails
fundamental interval: 38.5 W (nominal)
self-heating: 0.02 to 0.3 ºC/mW
thermal response: <0.4 s
measuring current: 1 mA
diameter: 1.5 mm
length: 15 mm
tolerance class (IEC 60751): Class A
temperature range: -200 ºC to +650 ºC
body material: alumina - adhesive-backed pad heater
power source: electric
voltage: max 60 V
power: max 59 W
resistance: 61 W
material: polyimide
maximum temperature: 250 ºC
wire type: silicone braided wire
insulating resistance: >5 MW
size: 50 mm x 50 mm
thickness: <0.2666 mm
adhesive: 3M
wire length: 60 mm - fittings
body material: Stainless Steel 316
connection 1 size: 1/4 in. tube OD (6.35 mm)
connection 1 type: Swagelok® Tube Fitting
connection 2 size: 7/16-20 in.
connection 2 type: male SAE/MS straight thread
reference: Swagelok® part #: SS-400-5-4ST
Intrastat data:
HS Code: 90278080
Country of Origin: Sweden
NET weight: 2000 g
List of Materials:
anode flow field (PEM): platinum coated titanium (grade II)
cathode flow field (PEM): gold coated titanium (grade II)
anode flow field (AEM): pure nickel
cathode flow field (AEM): pure nickel
threaded end plate: anodized aluminium
unthreaded end plate: anodized aluminium
current collectors: gold coated (nickel interlayer) copper (101)
fittings: Stainless Steel 316
bolts: zinc yellow-chromate plated steel grade 8
gaskets: skived PTFE and FKM
washers: Stainless Steel18/8
Belleville washers: Stainless Steel 302
insulating tape: PEEK
alignment pins: PFA
temperature sensor body: alumina
adhesive backed pad heater: polyimide with 3M adhesive
Setup includes:
1 x anode flow field
1 x cathode flow field
1 x threaded end plate
1 x unthreaded end plate
2 x current collector
4 x Swagelok® part #: SS-400-5-4ST fitting
8 x bolt
10 x FKM gasket
10 x skived PTFE gasket
16 x washer
64 x Belleville washer
2 x insulating PEEK tape
4 x alignment pin 11 mm long, 3 mm OD
2 x alignment pin 8 mm long, 3 mm OD
2 x dual Pt100 temperature sensor
2 x adhesive backed pad heater
Select configuration
Wrubel, Jacob, Samantha Ware, Corey Schaffer, Matt Allen, Ellis Klein, Robin Rice, Chaiwat Engtrakul, and Guido Bender. 2023. “NREL 25-cm2 High-Pressure Low-Temperature Electrolysis Cell Hardware (Open Source).” NREL Data Catalog. Golden, CO: National Renewable Energy Laboratory. https://doi.org/10.7799/2205626
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High-Pressure EC, 25 bar, 50 mL – High-Pressure Single-Compartment Electrochemical Cell (redox.me)
Read moreThe High-Pressure Electrochemical Cell is a sophisticated apparatus engineered to facilitate advanced research in electrochemistry under elevated pressure and temperature conditions. The cell is capable of withstanding pressures up to 25 bar and temperatures up to 200 ⁰C, allowing researchers to investigate electrochemical processes under hydrothermal conditions or using a hot pressurized environment for organic solvents as reaction media. It is a single-compartment cell that accommodates various electrode setups, including standard 2- or 3-electrode configurations and custom arrangements tailored to specific experimental requirements. The cell is designed to accommodate various electrodes and sample types, including solids, liquids, and gases, enabling comprehensive studies across different material systems.
The cell is constructed from high-quality materials such as Stainless Steel 316L (outer body), PEEK (liner), and FFKM elastomer (O-rings), ensuring robustness and reliability even under harsh experimental conditions. Cell material system is compatible with the following material systems: aqueous electrolytes in a full pH range, organic solvents (sulfoxides, amides, ethers, alcohols, aromatic), organic and inorganic salts (including fluorinated anions, ammonium), gases (N2, Ar, H2) – PEEK, FFKM O-Rings The cell is equipped with three 6 mm dia. electrode ports, two 1/4 in. OD tube gas/liquid inlet/outlet, and assembly of a manometer and safety relief valve (25 bar) mounted on the cooling tower. Additionally, there is a 1/8 in. OD port for a temperature probe inside the PEEK liner. The cell is compatible with the high-pressure working electrode, high-pressure counter electrode, and high-pressure reference electrode. Unused electrode ports can be terminated with high-pressure plug.Application note:
Catalysis plays a pivotal role in various industrial processes, from petroleum refining to pharmaceutical synthesis. Understanding catalytic mechanisms under realistic conditions is crucial for optimizing catalyst performance and developing efficient processes. The High Pressure Electrochemical Cell offers a sophisticated platform for studying catalytic reactions under elevated pressure and electrochemical environments simultaneously. The cell is typically used to investigate the effect of pressure on electrochemical kinetics and mechanisms, study the electrochemical behavior of materials under high-pressure conditions for applications in energy storage, catalysis, and corrosion, and explore novel electrode materials and electrolyte systems tailored for high-pressure electrochemical devices.
Electrodes are not included in the cell and should be added to the quotation separately.Specification:
maximum operating pressure: 25 bar
total volume of PEEK liner: 50 mL
recommended volume of liquid: 30 – 35 mL
maximum operating temperature: 200 ⁰C
port for temperature probe: 1/8 in. (3.175 mm)
electrode port diameter: 6 mm
number of electrode ports: 3
other port diameters: 1/4 in. (6.35 mm)
pressure gauge dial range: 0 – 40 bar
recommended tubing: 1/4 in. OD, 1/8 in. ID PEEK tubeIntrastat data:
HS Code: 90309000
Country of Origin: Sweden
NET weight: 2500gSafety note:
The use of a High-Pressure Electrochemical Cell involves working with equipment capable of withstanding elevated pressures and conducting experiments with potentially reactive chemicals. Ensuring safety during operation is paramount to prevent accidents and protect personnel and equipment. Below are key safety considerations to observe when using the High-Pressure Electrochemical Cell:1. Prior to operation, all personnel involved should receive comprehensive training on the setup, operation, and safety protocols associated with the High-Pressure Electrochemical Cell. Only trained individuals familiar with the equipment should be permitted to operate it.
2. Adhere strictly to the specified pressure limitations of the High-Pressure Electrochemical Cell. Do not exceed the recommended pressure range to prevent over-pressurization, which could lead to equipment failure and potential hazards.
3. Ensure that all materials, including electrodes, seals, and electrolytes, are compatible with the pressure and chemical environment inside the cell. Incompatibilities could result in leaks, corrosion, or other safety hazards.
4. Verify that the pressure relief mechanism is in place and functioning correctly. This mechanism is crucial for safely releasing excess pressure in the event of over-pressurization.
5. Regularly inspect the seals and connections of the High-Pressure Electrochemical Cell for signs of wear, damage, or leaks. Replace any compromised components promptly to maintain sealing integrity and prevent pressure-related accidents.
6. Establish clear emergency procedures, including evacuation routes and protocols for handling pressure-related incidents. Ensure that all personnel are aware of these procedures and know how to respond effectively in case of emergencies.
7. Wear appropriate Personal Protective Equipment (PPE), including safety glasses, gloves, and lab coats, when operating the High Pressure Electrochemical Cell. Additional PPE may be necessary depending on the specific experimental conditions and hazards involved.
8. Supervise experiments closely and monitor the High-Pressure Electrochemical Cell continuously during operation. Respond promptly to any abnormalities or unexpected changes in pressure or performance.
By adhering to these safety guidelines and exercising caution and diligence, users can minimize risks and ensure the safe and effective operation of the High-Pressure Electrochemical Cell in the laboratory. Always prioritize safety to protect yourself, your colleagues, and the integrity of the experimental setup.
Product includes:
1 x pressure vessel, SS 316L
1 x PEEK liner 50 mL
1 x PEEK lid
1 x set of PEEK screws
1 x cell lid, SS 316L
1 x screw cup, SS 316L
1 x cooling tower, SS 316L
1 x manometer (0 – 40 bar)
1 x safety relief valve set for 25 bar
1 x 4-way union, Swagelok 1/4 in. OD, SS 316L
3 x electrode fitting, Swagelok 6 mm OD x 1/8 in. Male NPT, SS 316L
2 x fitting, Swagelok 1/4 in. OD x 1/8 in. Male NPT, SS 316L
2 x ball valve, Swagelok 1/4 in. OD, SS 316L
1 x set of O-rings, FFKM,
1 x temperature probe fitting, IDEX, 1/8 in. x 1/4-28, SS 316L
3 x connecting unit, 1/4 in. OD, 1/8 in. ID, 30 mm long, SS 316L
2 x C-spanner 85 mm (cell opening tool)
1 x PEEK plug, 6 mm dia.
1 x PTFE tapeRelated products:
High-pressure working electrode
High-pressure counter electrode
High-pressure reference electrode
High-pressure plug
Related products
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Standard electrochemical cell setup (redox.me)
Read moreThis is a stationary solution standard electrochemical (electrolytic) cell for measurements of electrodes in a form of:
a) rod/disc (6 mm dia.),
b) thin film deposited on a flat substrate (using a sample holder) and
c) free-standing membrane (using the basic sample holder).
The working, counter, and reference electrodes are mounted in a top casing either in 2-, or 3-electrode setup. The cell has two spare ports for connection of e.g. thermometer, Clark electrode, pH meter electrode, or other 6 mm dia. electrode/probe.
The cell elements are constructed with materials that are inert to the sample (glass and PEEK). It well fits aqueous (EPDM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. The construction is gas-tight and can be used when the removal and exclusion of contaminants such as oxygen and water is required by bubbling of an inert gas through the electrolyte. The jacketed model is available here.
Application note
The reference electrode tip should be placed close to a working electrode center. This will ensure a low potential drop throughout the electrolyte solution for low-current experiment. Various auxiliary electrodes are suitable for this cell including metal wire and metal foil electrodes as well as graphite rod. The bubbling of gas through the solution must be stopped prior to experiment.Specification:
maximum electrolyte volume: 100, 150, 200, 250, 350, 500 or 1000 mL
electrode plug diameter: 6 mm
number of electrode ports: 5
vial material: borosilicate 3.3 glassIntrastat data:
HS Code: 90309000
Country of Origin: Sweden
NET weight: 200 g (100, 150 mL), 300 g (200, 250, 350 mL), 400 g (500 mL), 600 g (1000 mL) -
Platinum Coated Titanium Mesh Electrode with Holder – set of 10 pcs (redox.me)
Read moreThe metal counter (auxiliary) electrode is provided in electrochemical cell as a current sink to shunt excess current away from the reference electrode. Platinum Coated Titanium Mesh Electrode is a cheap alternative to pure Platinum Electrodes like Platinum Gauze Electrode or Metal Wire Auxiliary Electrode. Platinum coating makes this counter electrode inert under the reaction conditions and provides catalytic properties. The electrode is installed in the Basic Sample Holder (1 pcs included in the set), which allows full immersion of the electrode in the electrolyte (wet Tantalum contact). It well fits aqueous and organic solvent electrolyte requirements. Electrode size is customizable.
Application note
The Platinum Coated Titanium Mesh Electrode is fully immersed in the ion-conducting solution as a counter electrode. An electric current is passed between the working electrode and the Platinum Coated Titanium Mesh Electrode for a certain amount of time. After the process, the electrode should be washed several times with ethanol and dried under the nitrogen flow. Store the electrode in a dedicated compartment to avoid scratching. Discoloration may indicate the degradation (dissolution) of the Platinum layer and oxidation of Titanium mesh.
This electrode is used mainly in systems where there is a high risk of its contamination by organic or inorganic deposit during the electrochemical reaction. It is also a cheap replacement for pure Platinum electrode in electrodeposition processes.Specification
Titanium grade: GR1
working current: <5000 A/m2
Platinum content: >15 g/m2
Platinum coating thickness: 760 – 1500 nm
mesh hole size: 3 mm x 2 mm
mesh thickness: 0.5 mm
electrode size: 25x25mm2, 50x50mm2, 100x100mm2, custom
pH range: 1-12Intrastat data
HS Code: 71151000
Country of Origin: Sweden
NET weight: 100 gProduct includes
10 x Platinum Coated Titanium Mesh Electrode of selected size
1 x Basic Sample Holder (if selected) -
Modular PEM Electrolyzer Test Station up to 3 kW (redox.me)
Read moreThe Modular PEM Electrolyzer Test Station is a versatile and flexible solution designed for the testing and evaluation of proton exchange membrane (PEM) electrolyzers. Unlike fully automated, integrated systems, this platform features modular components that can be easily swapped by the end user, allowing for customized setups and adaptability to different testing needs. The platform is engineered to provide precise control and measurement of electrochemical performance while offering the convenience of easily replaceable parts.
This design enables users to test various configurations, integrate new modules, and adapt the system to specific research or development objectives without the need for specialized equipment or extensive downtime. Ideal for research labs and development environments, this platform supports the advancement of PEM electrolyzer technology through hands-on, flexible experimentation.
Application note:
Ideal for researchers investigating new PEM materials, flow field designs, and cell configurations. The system is an excellent tool for academic institutions and training centers, providing students and researchers with a hands-on understanding of PEM electrolysis processes and system operation. PEM Electrolyzer Test Station with power up to 3 kW is suitable for testing lab-scale or small to medium-scale electrolyzers, typically up to 60 cm². If the power requirements for a given electrolyzer are less than 2 A/cm², larger electrolyzers up to 100 cm² or more can also be tested.
The entire system, as well as its component parts, are CE certified, which signifies that a product meets European Union (EU) health, safety, and environmental protection standards. Other certificates are available upon request.The Modular PEM Electrolyzer Test Station is continuously being improved, so the photos may not fully represent the current version of the device.
Specification:
weight: 150 kg
height: 129 cm (25U)
width: 135 cm (85 cm with folded monitors)
depth: 90 cm
maximum input power: 3 kW
maximum input current: 120 A
maximum input volatge: 60 V
power connection: 230V, 3 kW, single phaseIntrastat data:
HS Code: 85433000
Country of Origin: Sweden
NET weight: 150 kgSetup includes:
1 x Modular PEM Electrolyzer Test Station or selected module(s) -
Metal Wire Auxiliary Electrode – 50HX15 0.6/250 mm (redox.me)
Read moreThe metal wire counter (auxiliary) electrode is provided in the electrochemical cell as a current sink to shunt excess current away from the reference electrode. The counter electrode is generally chosen to be inert under reaction conditions, typically platinum, rhodium, palladium, or gold wire. It well fits aqueous (FKM O-Ring) and organic solvent (FFKM O-Ring) electrolyte requirements.
Application note
The metal wire electrode is immersed in the ion-conducting solution as a counter electrode. An electric current is passed between the working electrode and the counter electrode for a certain amount of time. After the process, the electrode should be washed several times with isopropanol or ethanol and dried under the nitrogen flow. Store the metal wire electrode in the glass vial sealed with O-rings (all included in the package).Specification
helix inner diameter: 4.8 mm
helix outer diameter: 6 mm
number of turns: 12
wire diameter: 0.6 mm
total wire length: 250 mm (215 mm long helix, 35 mm long straight wire)Intrastat data
HS Code: 71101910 (platinum), 71081310 (gold),
Country of Origin: Sweden
NET weight: 100 gProduct includes
1 metal wire electrode with PEEK plug and selected electrical connector
1 O-Ring
1 glass vial












