Raman Electrochemical Flow Cell, active area: 3.5 cm2, volume: 4.5 mL (redox.me)

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  Bottom mount front contact electrochemical cell setup (redox.me)

  This is a static voltammetry cell with variants for different sample dimensions. The sample is loaded from the bottom via magnetic or screw mount, while counter or/and reference electrodes are mounted in the lid as either 2-, or 3-electrode configuration. The cell is constructed with materials that are inert to the sample environment (glass and PEEK), and it can be used with FKM/EPDM O-rings or FFKM O-rings for aqueous or organic electrolyte requirements, respectively. The construction is gas-tight and inert gas can be bubbled through the electrolyte to remove and exclude contaminants such as air or water.

   

  Application note:
  The reference electrode tip should be placed close to the sample surface to ensure a negligible potential drop throughout the electrolyte solution during low-current experiments. In the magnetic variant of the cell, the strength with which the magnets hold the sample is adjusted by adding or removing the washers under the magnets. Thanks to this procedure, the distance between the magnets changes, with it, the force of their attraction. Various auxiliary electrodes are suitable for this cell, including metal wire and metal plate electrodes as well as carbon-based electrodes (graphite or Glassy Carbon). If a purge gas is used, stop the flow during experiments for better results. 

   

  Specification:
  nominal exposure area: 0.07 cm² for 5x5mm², 0.2 cm² for 7x7mm², 0.5 cm² for 10x10mm², and 1.33 cm² for 15x15mm²
  minimum electrolyte volume: 2.5 mL
  maximum electrolyte volume: 15 mL
  electrode plug diameter: 6 mm
  substrate size: 5x5mm², 7x7mm², 10x10mm², and 15x15mm², other sizes available on request
  minimum substrate thickness: 0.4 mm*

  *lower thicknesses are also feasible when using a pad below the sample

   

  Intrastat data:
  HS Code: 90309000
  Country of Origin: Sweden
  NET weight: 200 g

   

  Setup includes:
  1 x BM FC EC 15mL – Bottom Mount Front Contact Electrochemical Cell, 15mL (or BMM FC EC 15mL – Bottom Magnetic Mount Front Contact Electrochemical Cell, 15mL)
        1 x lid
        1 x glass chamber
        1 x bottom casing
        1 x sample mount
        1 x tantalum contact
        1 x plug
        1 x set of Nylon screws (screw variant only)
  1 x Reference electrode (Ag/AgCl, or Ag/Ag+), 70mm, 4 mm female banana socket
  1 x Metal Wire Auxiliary Electrode – 50HX15 0.6/250 mm, platinum 99.9%, 4 mm female banana socket

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  Standard electrochemical cell setup (redox.me)

  This is a stationary solution standard electrochemical (electrolytic) cell for measurements of electrodes in a form of:

  a) rod/disc (6 mm dia.),

  b) thin film deposited on a flat substrate (using a sample holder) and

  c) free-standing membrane (using the basic sample holder).

   

  The working, counter, and reference electrodes are mounted in a top casing either in 2-, or 3-electrode setup. The cell has two spare ports for connection of e.g. thermometer, Clark electrode, pH meter electrode, or other 6 mm dia. electrode/probe. 

  The cell elements are constructed with materials that are inert to the sample (glass and PEEK). It well fits aqueous (EPDM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. The construction is gas-tight and can be used when the removal and exclusion of contaminants such as oxygen and water is required by bubbling of an inert gas through the electrolyte. The jacketed model is available here. 

   

  Application note
  The reference electrode tip should be placed close to a working electrode center. This will ensure a low potential drop throughout the electrolyte solution for low-current experiment. Various auxiliary electrodes are suitable for this cell including metal wire and metal foil electrodes as well as graphite rod. The bubbling of gas through the solution must be stopped prior to experiment.

   

  Specification:
  maximum electrolyte volume: 100, 150, 200, 250, 350, 500 or 1000 mL
  electrode plug diameter: 6 mm
  number of electrode ports: 5
  vial material: borosilicate 3.3 glass

   

  Intrastat data:
  HS Code: 90309000
  Country of Origin: Sweden
  NET weight: 200 g (100, 150 mL), 300 g (200, 250, 350 mL), 400 g (500 mL), 600 g (1000 mL)

   

   

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  AC1.GP. Electrochemical sensor with a working electrode of guaranteed purity

  Basic amperometric three-electrode sensor with patented structure made by thick film technology.

   

  Dimensions: 25.40 mm x 7.26 mm x 0.63 mm

  WE material: gold, platinum, silver, copper, iron, nickel, cobalt, chromium, tantalum, irridium, rhenium, magnesium, palladium, zirconium and others

   

  *Selection of sensor electrode materials other than those listed above is possible upon agreement with the customer.

   

   

  The sensor is made on a corundum ceramic base. Working, reference and auxiliary electrodes are applied to this surface. Working, reference and auxiliary electrodes are made of different materials. At the end of the sensor there is a contact field that is connected to the active part by silver conductive paths that are covered with a dielectric protective layer. The working electrode of the sensor with a diameter of 2 mm is made of a material of guaranteed purity of up to 99.99 % depending on the selected material– standard layer thickness 0.0125 mm.

   

   

  We also offer a working electrode made of polished gold AC1P.W*.R*, with homogenous surface with roughness less than 1 µm.

   

  We also offer activated graphite sensors on customer request.

   

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  ZIVE SP1 – potentiostat/galvanostat/ZRA

  • Potentiostat/galvanostat/ZRA at affordable price
  • Control voltage range: ±10V
  • Control current range:9 ranges, 10nA~1A (10nA with gain)

   

  Application Battery Super capacitor Fuel cell Corrosion Sensor Solar cell Other Echem experiments Features economical high quality potentiostat/galvanostat/impedance analyzer compact size with full functions ±10V@1Amp control range wide current ranges(1A to 10nA) for various applications built-in FRA : enables EIS tests by using software 14 EIS techniques capability including multisine capable of multitude of applications – corrosion, general electrochemistry, sensor, battery, fuel cell, supercapacitor, solar cell, etc. bipolar pulse capability voltage pulse or current pulse charge/discharge test(GSM,CDMA etc.), sine wave function for ripple simulation withenergysoftwarepackage & pulse plating available high speed data sampling time – 2usec or 3usec depending on data point number iR compensation and measurement 3 measurement/control voltage ranges & 9 measurement/control current ranges internal 542,000 data point storage & continuing experiment regardless of PC failure. multichannel configuration available free software upgrade Experimental Techniques Basic techniques Potentiostatic Galvanostatic Double step potentiostatic Double step galvanostatic OCP measurement Potential sweep Current sweep Cyclic voltammetry Fast potential sweep Potentiostatic Ru measurement Galvanostatic Ru measurement Advanced Software Package(Included) EIS software package(EISe) – Potentiostat EIS – Galvanostatic EIS – Pseudo galvanostatic EIS – OCP* EIS – Potentiodynamic PEIS – Galvanodynamic GEIS – Poteniodynamic HFR – Galvanodynamic HFR – Potentiostatic HFR monitor – Galvanostatic HFR monitor – Multisine potentiostatic EIS – Multisine galvanostatic EIS – Intermittent potentiostatic EIS – Intermittent galvanostatic EIS (*) The system measures open circuit potential before each frequency change and applies AC sine wave on this potential. Corrosion software package(CORe) – Tafel(Tafel experiment) – Rp(Polarization resistance) – RpEc trend – PDYN(Potentiodynamic) – CYPOL(Cyclic polarization resistance) – GDYN(GalvanoDynamic) – Reactivation – Galvanic corrosion – Potentiostatic ECN – Galvanostatic ECN – ZRA mode ECN Energy software package(BATe) a) Battery test technique – CC/CV testforcycle life test of lithium battery – CC/CC tet forcyclelifetestofNiCd or NiMH battery – Discharging test – EVS(electrochemical voltage spectroscopy) – Variable scan rate CV – Potentiostatic IV curve – Galvanostatic IV curve – Steady state CV – PITT(Potentiostatic intermittent titration technique) test – GITT(Galvanostatic intermittent titration technique) test – Pulse mode is available for GSM & CDMA profile. Pulse shape profile can be measured by user’s demand. b) Control mode – Charge : CC, CC-CV, pulse, sine wave – Discharge : CC, CP, CR, pulse, sine wave c) Cut-off condition – Time, voltage, current, power, auxV etc. – Various battery charge/discharge test is available including pulse discharge for GSM, CDMA application Electrochemical analysis software package(EASe) a) Step techniques – CA(Chronoamperometry) – CC(Chronocoulometry) – CP(Chronopotentiometry) b) Sweep techniques – LSV(Linear sweep voltammetry) – SDV(Sampled DC voltammetry) – Fast CV – Fast LSV c) Pulsed techniques – DPV(Differential pulse voltammetry) – SWV(Square wave voltammetry) – DPA(Diff.pulse amperometry) – NPV(Normal pulse voltammetry) – RNPV(Reverse normal pulse voltammetry) – DNPV(Differential normal pulse voltammetry)

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