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Sample Holder 25 mm x 25 mm (redox.me)
The sample holder (known also as flat specimen holder) is used for holding flat, circular or square/rectangular samples. It enables contacting the sample from the front (e.g. ITO/FTO glass, Monolayer Graphene on SiC, or Boron-Doped Diamond thin film on various substrates) and from the back (e.g. metal specimen, Glassy Carbon plate, Boron-Doped Diamond plate). The default nominal aperture is 1cm2, but other value can be provided on request. The large electrical contact with Tantalum (formerly Copper) foil surface (not being in contact with an electrolyte) ensures optimal current collection by minimizing electrical resistance and unifying current distribution. The rod with electrical connection has a diameter of 6 mm, which makes the sample holder compatible with our voltammetry cells and jacketed cells, as long as it fits in. We may also provide an adapter to install this sample holder in openings larger than 6 mm dia.
The sample holder elements are constructed with materials that are inert to the electrochemical system (PEEK, Fluorocarbons). It well fits aqueous (FKM/EPDM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. The construction is well sealed which prevents the electrolyte to leak inside.
Application note
The sample holder is used largely for corrosion studies. It can be installed in a beaker type cell as well as in testing environments such as open water reservoirs, cans, tanks etc. It can also be used wherever it is necessary to make an electrode using a thin layer of an active material deposited on a flat substrate (conducting or insulating).
Specification
nominal aperture range: 0.008 cm2 (1 mm dia.) – 4.155 cm2 (23 mm dia.)
minimum aperture: 0.008 cm2 (1 mm dia.)
maximum aperture: 4.9 cm2 (23 mm dia.)
electrical connection diameter (rod): 6 mm
minimum substrate size:
| nominal aperture | minimum substrate size |
| 0.008 cm2 (1 mm dia.) | 10 x 10 mm2 (square) or 12 mm dia. (circular). |
| 0.196 cm2 (5 mm dia.) | 7 x 7 mm2 (square) or 10 mm dia. (circular). |
| 0.283 cm2 (6 mm dia.) | 8 x 8 mm2 (square) or 11 mm dia. (circular). |
| 0.385 cm2 (7 mm dia.) | 9 x 9 mm2 (square) or 12 mm dia. (circular). |
| 1 cm2 (11.3 mm dia.) | 13 x 13 mm2 (square) or 16 mm dia. (circular). |
| 1.76 cm2 (15 mm dia.) | 17 x 17 mm2 (square) or 20 mm dia. (circular). |
| 3 cm2 (19.5 mm dia.) | 22 x 22 mm2 (square) or 24 mm dia. (circular). |
| 3.5 cm2 (21 mm dia.) | 23 x 23 mm2 (square) or 25 mm dia. (circular). |
| 4.155 cm2 (23 mm dia.) | 25 x 25 mm2 (square only) |
maximum substrate size: 25 x 25 mm2
maximum sample thickness: 4 mm
contact type: front or back
Intrastat data
HS Code: 90309000
Country of Origin: Sweden
NET weight: 100 g
Product includes
1 x chamber
1 x lid
1 x contact (Tantalum foil)
1 x rod with electrical connection
Select configuration
Operating Video Manual:
Related products
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ZIVE SP1 – potentiostat/galvanostat/ZRA
Read more- Potentiostat/galvanostat/ZRA at affordable price
- Control voltage range: ±10V
- Control current range:9 ranges, 10nA~1A (10nA with gain)
Application - Battery
- Super capacitor
- Fuel cell
- Corrosion
- Sensor
- Solar cell
- Other Echem experiments
Features
- economical high quality potentiostat/galvanostat/impedance analyzer
- compact size with full functions
- ±10V@1Amp control range
- wide current ranges(1A to 10nA) for various applications
- built-in FRA : enables EIS tests by using software
- 14 EIS techniques capability including multisine
- capable of multitude of applications
– corrosion, general electrochemistry, sensor, battery, fuel cell,
supercapacitor, solar cell, etc. - bipolar pulse capability
- voltage pulse or current pulse charge/discharge test(GSM,CDMA etc.),
sine wave function for ripple simulation withenergysoftwarepackage
& pulse plating available - high speed data sampling time
– 2usec or 3usec depending on data point number - iR compensation and measurement
- 3 measurement/control voltage ranges &
9 measurement/control current ranges - internal 542,000 data point storage & continuing experiment regardless
of PC failure. - multichannel configuration available
- free software upgrade
Experimental Techniques
Basic techniques
- Potentiostatic
- Galvanostatic
- Double step potentiostatic
- Double step galvanostatic
- OCP measurement
- Potential sweep
- Current sweep
- Cyclic voltammetry
- Fast potential sweep
- Potentiostatic Ru measurement
- Galvanostatic Ru measurement
Advanced Software Package(Included)
- EIS software package(EISe)
– Potentiostat EIS
– Galvanostatic EIS
– Pseudo galvanostatic EIS
– OCP* EIS
– Potentiodynamic PEIS
– Galvanodynamic GEIS
– Poteniodynamic HFR
– Galvanodynamic HFR
– Potentiostatic HFR monitor
– Galvanostatic HFR monitor
– Multisine potentiostatic EIS
– Multisine galvanostatic EIS
– Intermittent potentiostatic EIS
– Intermittent galvanostatic EIS
(*) The system measures open circuit potential before each frequency
change and applies AC sine wave on this potential. - Corrosion software package(CORe)
– Tafel(Tafel experiment)
– Rp(Polarization resistance)
– RpEc trend
– PDYN(Potentiodynamic)
– CYPOL(Cyclic polarization resistance)
– GDYN(GalvanoDynamic)
– Reactivation
– Galvanic corrosion
– Potentiostatic ECN
– Galvanostatic ECN
– ZRA mode ECN - Energy software package(BATe)
a) Battery test technique
– CC/CV testforcycle life test of lithium battery
– CC/CC tet forcyclelifetestofNiCd or NiMH battery
– Discharging test
– EVS(electrochemical voltage spectroscopy)
– Variable scan rate CV
– Potentiostatic IV curve
– Galvanostatic IV curve
– Steady state CV
– PITT(Potentiostatic intermittent titration technique) test
– GITT(Galvanostatic intermittent titration technique) test
– Pulse mode is available for GSM & CDMA profile.
Pulse shape profile can be measured by user’s demand.
b) Control mode
– Charge : CC, CC-CV, pulse, sine wave
– Discharge : CC, CP, CR, pulse, sine wave
c) Cut-off condition
– Time, voltage, current, power, auxV etc.
– Various battery charge/discharge test is available including
pulse discharge for GSM, CDMA application - Electrochemical analysis software package(EASe)
a) Step techniques
– CA(Chronoamperometry)
– CC(Chronocoulometry)
– CP(Chronopotentiometry)
b) Sweep techniques
– LSV(Linear sweep voltammetry)
– SDV(Sampled DC voltammetry)
– Fast CV
– Fast LSV
c) Pulsed techniques
– DPV(Differential pulse voltammetry)
– SWV(Square wave voltammetry)
– DPA(Diff.pulse amperometry)
– NPV(Normal pulse voltammetry)
– RNPV(Reverse normal pulse voltammetry)
– DNPV(Differential normal pulse voltammetry)
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Basic Sample Holder – metal contact, 4 mm max. thickness (redox.me)
Read moreBasic Sample Holder with a metal contact works as an electrical conductor between an electrode material (free-standing or deposited on a substrate) and an external circuit. This holder consists of PEEK body, pure Tantalum, Stainless Steel 316L, Titanium, Copper or Nickel metal electrical contact, and PEEK screw to fix the electrode. It is compatible with most of inorganic and organic based plates, free-standing membranes or thin films deposited on flexible and rigid substrates. A maximum thickness of the sample is 4 mm. Tantalum is known to be inert to practically all organic and inorganic compounds. Tantalum’s corrosion resistance is very similar to that of glass, as both are unsuitable for use in hydrofluoric acid and strong hot alkali applications. Therefore, in those cases, we recommend the other wire contact variant. The metal contact can be fully immersed in the electrolyte.
Application note
Generally, the electrode is fabricated by fixing the electrochemical active sample into the holder using a screw. Such electrode is immersed in the ion-conducting solution as a working electrode or counter electrode. An electric current is passed between the working electrode and the counter electrode for a certain amount of time. Metal wire contact is permanently installed in the PEEK body. The holder is designed to be used multiple times. The holder should be cleaned prior to the installation of electrode material.Specification
holder body material: PEEK
rod diameter: 6 mm
contact material: Ta, SS 316L, Ti, Cu or Ni
contact wire diameter: 0.6 mm
contact wire total length: 110 mm
holder length: 70 mm
maximum sample thickness: 4 mmIntrastat data
HS Code: 90309000
Country of Origin: Sweden
NET weight: 100 gProduct includes
1 x Basic Sample Holder
1 x PEEK M3 screw
1 O-Ring (FKM for aqueous or FFKM for organic electrolytes) -
Hanging Platinum Drop Electrode
Read moreThe Hanging Platinum Drop Electrode (HPDE) is solid phase alanogy of HMDE.
The drop of liquid Pt at 2000 °C forms a drop of Pt. The surface of HPDE has nearly ideal surface which is impossible to obtain using polishing. HPDE has also spherical symmetry which enables mathematical treatment of its response.
The material is not toxic and it is chemically stable. The only disadvantage is HPDE cleaning, which can be, however, in some cases solved by carefull insertion of the electrode tip to the flame of an alcohol burner.
Thus HPDE can be used as reference electrode for complicated electrochemical studies, where it is necessary to distinguish the analytical signal from the signal generated by surface inhomogenities.Hanging platinum drop electrode (HPDE) is designed for measurements with thermostated cell TC4, TC5, TC6 and TC9.
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Basic electrochemical cell setup (redox.me)
Read moreThis is a stationary solution basic electrochemical cell for measurements of electrodes in a form of:
a) rod/disc (6 mm dia.),
b) thin film deposited on a flat substrate (using a wire clip) and
c) membrane (using a wire clip).
The working, counter, and reference electrodes are mounted in a top casing either in 2-, or 3-electrode setup. The cell elements are constructed with materials that are inert to the sample (glass and PEEK). It well fits aqueous (FKM/EPDM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. The construction is gas-tight and can be used when the removal and exclusion of contaminants such as oxygen and water is required by bubbling of an inert gas through the electrolyte. The cell chamber is available in several material variants here (glass, PTFE, PEEK)
Application note:
The reference electrode tip should be placed at the level of working electrode center. This will ensure a low potential drop throughout the electrolyte solution for low-current experiment. Various auxiliary electrodes are suitable for this cell including metal wire and metal foil electrodes as well as graphite rod. The bubbling of gas through the solution must be stopped prior to experiment.Specification:
maximum electrolyte volume: 50 mL
electrode plug diameter: 6 mm
number of electrode slots: 3Intrastat data:
HS Code: 90309000
Country of Origin: Sweden
NET weight: 200 gSetup includes:
Item Qty B-A-BEC-50 B-O-BEC-50 BEC 50 mL – Basic Electrochemical Cell 1 C-A-BEC-50 C-O-BEC-50 Metal wire auxiliary electrode – 50HX15 0.6/250 mm, platinum (99,9%), 1 mm dia. gold plated pin 1 E-A-50HX15_Pt-1mm E-O-50HX15_Pt-1mm Silver / Silver Chloride Reference Electrode – Ag/AgCl 70 mm 1 E-Ag/AgCl_70 Non-aqueous Silver / Silver Ion Reference Electrode – Ag/Ag+ 70 mm 1 E-Ag/Ag+_70 Working disk electrode – 2 mm dia., PEEK BODY 6 mm dia. – 70 mm, glassy carbon 1 E-A-DISK_GC-70 E-O-DISK_GC-70 10 pcs of Tantalum wire clip with septum plug 0.6 mm dia., 60 mm long 1 E-A-Ta_CLIP-0.6/60-10p E-O-Ta_CLIP-0.6/60-10p








